Silver nanoparticles coated by Schiff base as an adsorbent of lead from polluted water.
DOI:
https://doi.org/10.56714/bjrs.49.1.4Keywords:
Adsorption, Schiff base, Silver nanoparticles, SEMAbstract
Synthesis of silver nanoparticles coated with Schiff base was achieved . Silver nanoparticles are reduced and coated using Schiff base. Schiff base serves as a capping to stop silver oxide from overgrowing. Schiff base produces silver nanoparticles with a novel form and a distinctive appearance. The presence of Schiff base as a reducing and capping agent can give a new shape for prepared silver nanoparticles. The structure of Schiff base was analyzed based on spectral data (1 H nuclear magnetic resonance (H1NMR), Mass spectroscopy, and Fourier-transform infrared spectroscopy (FTIR). The formation of silver nanoparticles within a surface plasmon band at 461 nm was observed using UV-Vis Spectroscopy. Silver nanoparticles with a spherical shape and a particle size between 50 and 100 nm are visible in a scanning electron microscope image. For the first time, silver nanoparticles coated with Schiff base were used to adsorb lead from a sample of polluted water. The rate of adsorption was 69%.
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Copyright (c) 2023 Ahmed M. Zaidan, Zainab T. Alabdullah, Uhood J. Al-Hamdani
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